2-[3-(9H-carbazol-9-yl)propyl]-1,3-bistosyloxypropane

Base Information

• Chemical Name: 2-[3-(9H-carbazol-9-yl)propyl]-1,3-bistosyloxypropane
• CAS No.: 1542616-09-0
• Molecular Formula: C₃₂H₃₃NO₆S₂
• Molecular Weight: 591.749
• Mol file: 1542616-09-0.mol

Synonyms:2-[3-(9H-carbazol-9-yl)propyl]-1,3-bistosyloxypropane

Chemical Property of 2-[3-(9H-carbazol-9-yl)propyl]-1,3-bistosyloxypropane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-[3-(9H-carbazol-9-yl)propyl]-1,3-bistosyloxypropane

There total 1 articles about 2-[3-(9H-carbazol-9-yl)propyl]-1,3-bistosyloxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-(3-bromopropyl)-9H-carbazole (84359-61-5) → 2-[3-(9H-carbazol-9-yl)propyl]-1,3-bistosyloxypropane (1542616-09-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium / ethanol / 8 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethanol / 12 h / 0 - 20 °C

3.1: sodium hydroxide / water; tetrahydrofuran / 0.5 h / 0 °C

3.2: 4 h / 20 °C

With sodium tetrahydroborate; sodium; sodium hydroxide; In tetrahydrofuran; ethanol; water;

DOI:10.1007/s11426-013-5031-5

upstream raw materials:

9-(3-bromopropyl)-9H-carbazole

Refernces