7-oxoheptanoic acid phenylamide

Base Information

• Chemical Name: 7-oxoheptanoic acid phenylamide
• CAS No.: 728890-58-2
• Molecular Formula: C₁₃H₁₇NO₂
• Molecular Weight: 219.283
• Mol file: 728890-58-2.mol

Synonyms:7-oxoheptanoic acid phenylamide

Chemical Property of 7-oxoheptanoic acid phenylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 7-oxoheptanoic acid phenylamide

There total 15 articles about 7-oxoheptanoic acid phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

C13H19NO2 (1377956-60-9) → 7-oxoheptanoic acid phenylamide (728890-58-2)

Guidance literature:

C₁₃H₁₉NO₂; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 - -60 ℃; for 1.08333h;

With triethylamine; In dichloromethane; at -60 - 20 ℃; for 2h;

DOI:10.1246/cl.130243

Reference yield: 72.0%

heptanedioic acid methoxymethylamide phenylamide (728890-57-1) → 7-oxoheptanoic acid phenylamide (728890-58-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

DOI:10.1016/j.bmcl.2004.03.063

Reference yield: 54.0%

6-(1,3-dioxolan-2-yl)-N-phenylhexanamide → 7-oxoheptanoic acid phenylamide (728890-58-2)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 70 ℃; for 3h;

DOI:10.1007/s10593-015-1752-z

upstream raw materials:

heptanedioic acid methoxymethylamide phenylamide

heptanedioic acid

7-oxo-7-(phenylamino)heptanoic acid

aniline