heptanedioic acid methoxymethylamide phenylamide

Base Information

Chemical Name:heptanedioic acid methoxymethylamide phenylamide
CAS No.:728890-57-1
Molecular Formula:C₁₅H₂₂N₂O₃
Molecular Weight:278.351
Hs Code.:

Synonyms:heptanedioic acid methoxymethylamide phenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of heptanedioic acid methoxymethylamide phenylamide

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Technology Process of heptanedioic acid methoxymethylamide phenylamide

There total 6 articles about heptanedioic acid methoxymethylamide phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 160777-08-2
7-oxo-7-(phenylamino)heptanoic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 728890-57-1
heptanedioic acid methoxymethylamide phenylamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmcl.2004.03.063

Reference yield: 85.0%

: 160777-08-2
7-oxo-7-(phenylamino)heptanoic acid

: 1117-97-1
N,0-dimethylhydroxylamine

: 728890-57-1
heptanedioic acid methoxymethylamide phenylamide

Guidance literature:: 7-oxo-7-(phenylamino)heptanoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

N,0-dimethylhydroxylamine; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

Reference yield:

: 111-16-0
heptanedioic acid

: 728890-57-1
heptanedioic acid methoxymethylamide phenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / 1 h / 180 °C

2: 94 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxy-1H-benzotriazole monohydrate; triethylamine / dimethylformamide / 20 °C

With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.04.002