2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose
CAS No.:522634-55-5
Molecular Formula:C₅₅H₆₃N₃O₁₃
Molecular Weight:974.118
Hs Code.:

Synonyms:2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

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Chemical Property of 2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

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Technology Process of 2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

There total 9 articles about 2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 522634-54-4
2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosylamine

: 522634-55-5
2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With hydrogenchloride; In methanol; chloroform; at 20 ℃;
DOI:10.1081/CAR-120016847

Reference yield:

: 29847-23-2
2-N-acetylamido-2-deoxy-β-D-glucopyranosyl azide

: 522634-55-5
2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 0 - 20 °C

1.2: 52 percent / BaO; Ba(OH)2*8H₂O / dimethylformamide; CH₂Cl₂ / Heating

2.1: 100 percent / hydrogen / PtO₂*nH₂O / ethanol / 2.5 h / 20 °C

3.1: 65 percent / molecular sieves (4 Angstroem); EDC; HOBt / NEt₃ / CH₂Cl₂ / 30 h / 20 °C

4.1: 93 percent / hydrogen / Pd/C / methanol / 0.58 h / 20 - 60 °C

5.1: 70 percent / aq. HCl / methanol; CHCl₃ / 20 °C

With hydrogenchloride; 4 A molecular sieve; hydrogen; sodium hydride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; platinum(IV) oxide; palladium on activated charcoal; triethylamine; In methanol; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120016847

Reference yield:

: 100-39-0
benzyl bromide

: 522634-55-5
2-acetamido-4-O-[3-[[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)amino]carbonyl]propanoyl]-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 0 - 20 °C

1.2: 52 percent / BaO; Ba(OH)2*8H₂O / dimethylformamide; CH₂Cl₂ / Heating

2.1: 100 percent / hydrogen / PtO₂*nH₂O / ethanol / 2.5 h / 20 °C

3.1: 65 percent / molecular sieves (4 Angstroem); EDC; HOBt / NEt₃ / CH₂Cl₂ / 30 h / 20 °C

4.1: 93 percent / hydrogen / Pd/C / methanol / 0.58 h / 20 - 60 °C

5.1: 70 percent / aq. HCl / methanol; CHCl₃ / 20 °C

With hydrogenchloride; 4 A molecular sieve; hydrogen; sodium hydride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; platinum(IV) oxide; palladium on activated charcoal; triethylamine; In methanol; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120016847