N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester

Base Information

Chemical Name:N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester
CAS No.:521286-12-4
Molecular Formula:C₁₇H₁₈N₄O₆
Molecular Weight:374.353
Hs Code.:

Synonyms:N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester

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Chemical Property of N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester

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Technology Process of N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester

There total 3 articles about N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 17763-80-3
para-nitrophenyl triflate

: 226065-33-4
tert-butyl 1-(4-nitrophenyl)hydrazinecarboxylate

: 521286-12-4
N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; caesium carbonate; In toluene; at 110 ℃; for 2h;
DOI:10.1021/ol027311u

Reference yield: 95.0%

: 636-98-6
p-nitrobenzene iodide

: 226065-33-4
tert-butyl 1-(4-nitrophenyl)hydrazinecarboxylate

: 521286-12-4
N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; caesium carbonate; In toluene; at 110 ℃; for 27h;
DOI:10.1021/ol027311u

Reference yield: 87.0%

: 586-78-7
para-nitrophenyl bromide

: 226065-33-4
tert-butyl 1-(4-nitrophenyl)hydrazinecarboxylate

: 521286-12-4
N'-(4-nitro-phenyl)-N-(4-nitro-phenyl)-hydrazine carboxylic acid tert-butyl ester

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; caesium carbonate; In toluene; at 110 ℃; for 30h;
DOI:10.1021/ol027311u