methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate

Base Information

Chemical Name:methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate
CAS No.:1003931-54-1
Molecular Formula:C₁₉H₁₉BrN₂O₆
Molecular Weight:451.274
Hs Code.:

Synonyms:methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate

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Chemical Property of methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate

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Technology Process of methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate

There total 2 articles about methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1003931-51-8
methyl 2-((benzyloxy)amino)-5-bromonicotinoate

: 36239-09-5
ethyl chlorocarbonylacetate

: 1003931-54-1
methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate

Guidance literature:: With triethylamine; In dichloromethane; for 1h;

Reference yield:

: 78686-79-0
methyl 2-chloro-5-bromonicotinate

: 1003931-54-1
methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 110 °C

1.2: pH 4 / Acidic aqueous solution

2.1: triethylamine / dichloromethane / 1 h

With triethylamine; In dichloromethane;

Reference yield:

: 1003931-54-1
methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate

: 1003931-57-4
ethyl 1-(benzyloxy)-6-bromo-4-hydroxy-2-oxo-1,2-dihydro-1,8-naphthyridine-3-carboxylate

Guidance literature:: methyl 2-[(benzyloxy)(3-ethoxy-3-oxopropanoyl)amino]-5-bromonicotinate; With sodium ethanolate; In ethanol; for 18h;

With hydrogenchloride; In ethanol; water; for 0.25h; pH=4;