4-methoxyphenyl dithiocarbamic acid triethylammonium

Base Information

• Chemical Name: 4-methoxyphenyl dithiocarbamic acid triethylammonium
• CAS No.: 43009-18-3
• Molecular Formula: C₆H₁₅N*C₈H₉NOS₂
• Molecular Weight: 300.489

Synonyms:4-methoxyphenyl dithiocarbamic acid triethylammonium

Chemical Property of 4-methoxyphenyl dithiocarbamic acid triethylammonium

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of 4-methoxyphenyl dithiocarbamic acid triethylammonium

There total 2 articles about 4-methoxyphenyl dithiocarbamic acid triethylammonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.3%

→ 4-methoxyphenyl dithiocarbamic acid triethylammonium (43009-18-3)

Guidance literature:

In diethyl ether; at 20 ℃; for 10h;

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 4-methoxy-aniline (104-94-9) + triethylamine (121-44-8) → 4-methoxyphenyl dithiocarbamic acid triethylammonium (43009-18-3)

Guidance literature:

In benzene; at 0 ℃; for 8h;

DOI:10.1016/0223-5234(89)90011-1

Reference yield: 98.0%

4-methoxyphenyl dithiocarbamic acid triethylammonium (43009-18-3) → 4-Methoxyphenyl isothiocyanate (2284-20-0)

Guidance literature:

With iodine; triethylamine; In acetonitrile; at 5 ℃; Cooling with ice;

DOI:10.1002/ejoc.200801270

upstream raw materials:

carbon disulfide

4-methoxy-aniline

triethylamine

Downstream raw materials:

4,5,6-triethyl-3-(4-methoxy-phenyl)-[1,3,5]thiadiazinane-2-thione

phenyl isothiocyanate

4-Methoxyphenyl isothiocyanate

4-(4-methoxy-phenyl)-5-phenylimino-[1,2,4]dithiazolidine-3-thione

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