(1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

Base Information

Chemical Name:(1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane
CAS No.:850888-42-5
Molecular Formula:C₂₈H₂₈FNO₅S
Molecular Weight:509.598
Hs Code.:

Synonyms:(1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

Suppliers and Price of (1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

Chemical Property:

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Technology Process of (1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

There total 5 articles about (1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1R)-2β-trifluoromethanesulfonyloxymethyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

: 533-31-3
Sesamol

: 850888-42-5
(1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

Guidance literature:: With sodium; In tetrahydrofuran; dichloromethane; at 20 ℃; for 14h;
DOI:10.1016/j.bmc.2005.01.046

Reference yield:

: 850888-41-4
(1R)-2β-hydroxymethyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

: 850888-42-5
(1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 1 h / -78 °C

2: 1.56 g / sodium / tetrahydrofuran; CH₂Cl₂ / 14 h / 20 °C

With pyridine; sodium; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2005.01.046

Reference yield:

: 850888-40-3
(1R)-2β-carbomethoxy-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

: 850888-42-5
(1R)-2β-[(3,4-methylenedioxy)phenoxy]methyl-3β-(4-fluorophenyl)-8-(4-methyl benzenesulfonyl)tropane

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

2: pyridine / CH₂Cl₂ / 1 h / -78 °C

3: 1.56 g / sodium / tetrahydrofuran; CH₂Cl₂ / 14 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sodium; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2005.01.046