(+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid

Base Information

Chemical Name:(+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid
CAS No.:132101-68-9
Molecular Formula:C₃₉H₄₀N₂O₅
Molecular Weight:616.757
Hs Code.:

(+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<<phenylmethoxy)carbonyl>amino>heptanoic acid

Synonyms:(+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid

Chemical Property:

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Technology Process of (+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid

There total 6 articles about (+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87905-98-4
5-<(benzyloxycarbonyl)amino>pentanol

: 132101-68-9
(+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / triethylamine (TEA) / CHCl₃ / 2 h / -20 °C

2: 1.) NaH, 2.) KI / 1.) DMSO, 2.) 5 d

3: aq. NaOH / dioxane; methanol / 3 h / Ambient temperature

4: toluene; dioxane / 4 h / Heating

With sodium hydroxide; sodium hydride; triethylamine; potassium iodide; In 1,4-dioxane; methanol; chloroform; toluene;
DOI:10.1021/jm00108a004

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 132101-68-9
(+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: aq. NaOH / dioxane / 48 h / Ambient temperature

2: 93 percent / triethylamine (TEA) / CHCl₃ / 2 h / -20 °C

3: 1.) NaH, 2.) KI / 1.) DMSO, 2.) 5 d

4: aq. NaOH / dioxane; methanol / 3 h / Ambient temperature

5: toluene; dioxane / 4 h / Heating

With sodium hydroxide; sodium hydride; triethylamine; potassium iodide; In 1,4-dioxane; methanol; chloroform; toluene;
DOI:10.1021/jm00108a004

Reference yield:

: 132101-95-2
1-Z-amino-5-<(methylsulfonyl)oxy>pentane

: 132101-68-9
(+/-)-2-<<3-(1-naphthalenyl)-2-(1-naphthalenylmethyl)-1-oxopropyl>amino>-7-<amino>heptanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH, 2.) KI / 1.) DMSO, 2.) 5 d

2: aq. NaOH / dioxane; methanol / 3 h / Ambient temperature

3: toluene; dioxane / 4 h / Heating

With sodium hydroxide; sodium hydride; potassium iodide; In 1,4-dioxane; methanol; toluene;
DOI:10.1021/jm00108a004