(RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid

Base Information

Chemical Name:(RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid
CAS No.:117997-60-1
Molecular Formula:C₂₂H₃₄ClN₃O₄
Molecular Weight:439.983
Hs Code.:

Synonyms:(RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid

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Chemical Property of (RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid

Chemical Property:

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Technology Process of (RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid

There total 4 articles about (RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 117997-61-2
4-[3-(4-Chloro-phenyl)-ureido]-4-dipentylcarbamoyl-butyric acid benzyl ester

: 117997-60-1
(RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran;
DOI:10.1021/jm00164a020

Reference yield:

: 117997-81-6
5-(benzyloxy)-2-(tert-butoxycarbonylamino)-5-oxopentanoic acid

: 117997-60-1
(RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 48 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / pH >8.5

2: 75 percent / HCl gas / ethyl acetate / 0.33 h / -25 °C

3: 84 percent / Et₃N / tetrahydrofuran / 24 h / Ambient temperature

4: 85 percent / 2.5 N NaOH / tetrahydrofuran

With hydrogenchloride; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/jm00164a020

Reference yield:

: 118100-26-8
N^α-Boc-ε-benzyl-DL-glutamic acid dipentylamide

: 117997-60-1
(RS)-4-[(4-chlorophenylaminocarbonyl)amino]-5-(dipentylamino)-5-oxo-pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / HCl gas / ethyl acetate / 0.33 h / -25 °C

2: 84 percent / Et₃N / tetrahydrofuran / 24 h / Ambient temperature

3: 85 percent / 2.5 N NaOH / tetrahydrofuran

With hydrogenchloride; sodium hydroxide; triethylamine; In tetrahydrofuran; ethyl acetate;
DOI:10.1021/jm00164a020