C₁₈H₈Cl₂F₁₀N₄

Base Information

Chemical Name:C₁₈H₈Cl₂F₁₀N₄
CAS No.:1334128-32-3
Molecular Formula:C₁₈H₈Cl₂F₁₀N₄
Molecular Weight:541.178
Hs Code.:

C<sub>18</sub>H<sub>8</sub>Cl<sub>2</sub>F<sub>10</sub>N<sub>4</sub>

Synonyms:C₁₈H₈Cl₂F₁₀N₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₈Cl₂F₁₀N₄

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Technology Process of C₁₈H₈Cl₂F₁₀N₄

There total 6 articles about C₁₈H₈Cl₂F₁₀N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1334128-64-1
1-[2,6-dichloro-4-(1,2,2,3,3,3-hexafluoro-1-(trifluoromethyl)propyl)phenyl]-4-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazole

: 1334128-32-3
C₁₈H₈Cl₂F₁₀N₄

Guidance literature:: 1-[2,6-dichloro-4-(1,2,2,3,3,3-hexafluoro-1-(trifluoromethyl)propyl)phenyl]-4-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazole; With hydrogenchloride; tin(ll) chloride; In water; isopropyl alcohol; at 0 - 80 ℃; for 2h;

With sodium hydroxide; In water; isopropyl alcohol; pH=8 - 9;

Reference yield:

: 364-73-8
4-Bromo-1-fluoro-2-nitrobenzene

: 1334128-32-3
C₁₈H₈Cl₂F₁₀N₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / triphenylphosphine; palladium diacetate / 4.25 h / 100 °C / Inert atmosphere; Reflux

2.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h / 20 °C

3.1: hydrogenchloride; tin(ll) chloride / isopropyl alcohol; water / 2 h / 0 - 80 °C

3.2: pH 8 - 9

With hydrogenchloride; triethylamine; tin(ll) chloride; copper(ll) sulfate pentahydrate; palladium diacetate; sodium L-ascorbate; triphenylphosphine; In water; isopropyl alcohol; tert-butyl alcohol;

Reference yield:

: 1207315-63-6
4-(1,2,2,3,3,3-hexafluoro-1-trifluoromethylpropyl)phenylamine

: 1334128-32-3
C₁₈H₈Cl₂F₁₀N₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / dichloromethane / 20 °C

2.1: hydrogenchloride / water / 0.5 h / 20 °C

2.2: 0.5 h / 0 - 5 °C

2.3: 0 - 20 °C

3.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h / 20 °C

4.1: hydrogenchloride; tin(ll) chloride / isopropyl alcohol; water / 2 h / 0 - 80 °C

4.2: pH 8 - 9

With hydrogenchloride; N-chloro-succinimide; tin(ll) chloride; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; isopropyl alcohol; tert-butyl alcohol;