N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

Base Information

Chemical Name:N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine
CAS No.:1609396-90-8
Molecular Formula:C₄₁H₃₁ClF₃NO₇S
Molecular Weight:774.214
Hs Code.:

Synonyms:N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

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Chemical Property of N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

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Technology Process of N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

There total 5 articles about N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 1609396-82-8
2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

: 1609396-90-8
N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

Guidance literature:: In toluene; at 155 - 160 ℃; for 10.25h;
DOI:10.1007/s12039-013-0551-2

Reference yield:

: 1609396-75-9
C₁₅H₁₂ClF₃N₂O₂S

: 1609396-90-8
N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

Guidance literature:: Multi-step reaction with 3 steps

1: 4 h / Reflux

2: potassium hydroxide / ethanol; acetone / 4.5 h / Reflux

3: toluene / 10.25 h / 155 - 160 °C

With potassium hydroxide; In ethanol; acetone; toluene; 2: |Smiles Aromatic Rearrangement;
DOI:10.1007/s12039-013-0551-2

Reference yield:

: 90382-10-8
2-amino-5-ethylbenzothiazole

: 1609396-90-8
N-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-2-chloro-7-ethyl-3-trifluoromethyl-10H-phenothiazine

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / ethanol / Reflux

2: 4 h / Reflux

3: potassium hydroxide / ethanol; acetone / 4.5 h / Reflux

4: toluene / 10.25 h / 155 - 160 °C

With sodium acetate; potassium hydroxide; In ethanol; acetone; toluene; 3: |Smiles Aromatic Rearrangement;
DOI:10.1007/s12039-013-0551-2