N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine

Base Information

Chemical Name:N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine
CAS No.:1219468-17-3
Molecular Formula:C₁₇H₁₆N₂O₂
Molecular Weight:280.326
Hs Code.:

Synonyms:N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine

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Chemical Property of N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine

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Technology Process of N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine

There total 1 articles about N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1219468-07-1
2-(2-bromoethyl)-4-methoxybenzaldehyde

: 613-94-5
benzoic acid hydrazide

: 1219468-17-3
N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine

Guidance literature:: 2-(2-bromoethyl)-4-methoxybenzaldehyde; benzoic acid hydrazide; In methanol; at 20 ℃; for 1.16667h; Reflux;

With triethylamine; In methanol; at 20 ℃; for 0.166667h; Further stages;
DOI:10.1021/ja100787a

Reference yield: 99.0%

: 1219468-17-3
N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine

: 536-74-3
phenylacetylene

: 1337924-67-0
C₂₅H₂₂N₂O₂

Guidance literature:: With copper diacetate; 2,6-bis[(4R)-5,5-dihydro-4-phenyl-2-oxazolyl]pyridine; In dichloromethane; at 0 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201104017

Reference yield: 95.0%

: 926-02-3
tert-butyl vinyl ether

: 1219468-17-3
N-benzoylimino-3,4-dihydro-6-methoxyisoquinolinium betaine

: 1304727-15-8
C₂₃H₂₈N₂O₃

Guidance literature:: With C₆₄H₄₂O₄; In chloroform; at -20 ℃; for 12h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.201100331