C₂₄H₂₇N₃O₆S

Base Information

• Chemical Name: C₂₄H₂₇N₃O₆S
• CAS No.: 1310050-48-6
• Molecular Formula: C₂₄H₂₇N₃O₆S
• Molecular Weight: 485.561
• Mol file: 1310050-48-6.mol

Synonyms:C₂₄H₂₇N₃O₆S

Chemical Property of C₂₄H₂₇N₃O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₇N₃O₆S

There total 6 articles about C₂₄H₂₇N₃O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C23H27N3O4S (1310050-47-5) + acetic anhydride (108-24-7) → C24H27N3O6S (1310050-48-6)

Guidance literature:

C₂₃H₂₇N₃O₄S; With trifluoroacetic acid; In water; at 20 ℃; for 0.166667h;

acetic anhydride; With dmap; triethylamine; In dichloromethane; for 0.5h;

DOI:10.1021/jo1025157

Reference yield:

C16H21N3O4S (1310050-46-4) → C24H27N3O6S (1310050-48-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

2.1: trifluoroacetic acid / water / 0.17 h / 20 °C

2.2: 0.5 h

With sodium hydride; trifluoroacetic acid; In water; N,N-dimethyl-formamide; mineral oil;

DOI:10.1021/jo1025157

Reference yield:

para-thiocresol (106-45-6) → C24H27N3O6S (1310050-48-6)

Guidance literature:

Multi-step reaction with 5 steps

1.1: boron trifluoride diethyl etherate / chloroform / 0 - 40 °C

2.1: sodium methylate / methanol / 0.5 h / 20 °C

2.2: Amberlite IR-120H(+) resin

3.1: camphor-10-sulfonic acid / 24 h / 20 °C / Inert atmosphere

3.2: Reflux

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

5.1: trifluoroacetic acid / water / 0.17 h / 20 °C

5.2: 0.5 h

With camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; trifluoroacetic acid; In methanol; chloroform; water; N,N-dimethyl-formamide; mineral oil;

DOI:10.1021/jo1025157

upstream raw materials:

C₁₆H₂₁N₃O₄S

C₂₃H₂₇N₃O₄S

acetic anhydride

1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-galactopyranose

Downstream raw materials:

3,4-di-O-acetyl-2-azido-6-O-benzyl-2-deoxy-α-D-galactopyranose 1-O-trichloroacetimidate

C₄₅H₄₅N₃O₁₅