Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

Base Information

Chemical Name:Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate
CAS No.:158535-93-4
Molecular Formula:C₃₀H₃₆O₈
Molecular Weight:524.611
Hs Code.:

Synonyms:Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

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Chemical Property of Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

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Technology Process of Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

There total 1 articles about Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 158535-92-3
Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-<(tert-butyldimethylsilyl)oxy>-2-(methoxymethoxy)hexanoate

: 158535-93-4
Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; acetic acid; for 20h; Ambient temperature;
DOI:10.1021/jo00091a034

Reference yield: 89.0%

: 158535-93-4
Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

: 158535-94-5
Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 0.333333h; Ambient temperature;
DOI:10.1021/jo00091a034

Reference yield:

: 158535-93-4
Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

: Methyl (methyl 2,3,4-tri-O-benzyl-α-L-idopyranoside)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Dess-Martin reagent / CH₂Cl₂ / 0.33 h / Ambient temperature

2: 61 percent / 12 M aq. HCl / methanol / 1.5 h / Heating

With hydrogenchloride; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1021/jo00091a034