Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate

Base Information

Chemical Name:Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate
CAS No.:158535-94-5
Molecular Formula:C₃₀H₃₄O₈
Molecular Weight:522.595
Hs Code.:

Synonyms:Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate

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Technology Process of Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate

There total 2 articles about Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 158535-93-4
Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-hydroxy-2-(methoxymethoxy)hexanoate

: 158535-94-5
Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 0.333333h; Ambient temperature;
DOI:10.1021/jo00091a034

Reference yield:

: 158535-92-3
Methyl (2R,3S,4R,5S)-3,4,5-tris(benzyloxy)-6-<(tert-butyldimethylsilyl)oxy>-2-(methoxymethoxy)hexanoate

: 158535-94-5
Methyl (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-(methoxymethoxy)-6-oxohexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / n-Bu₄NF / tetrahydrofuran; acetic acid / 20 h / Ambient temperature

2: 89 percent / Dess-Martin reagent / CH₂Cl₂ / 0.33 h / Ambient temperature

With tetrabutyl ammonium fluoride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1021/jo00091a034