4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide

Base Information

Chemical Name:4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide
CAS No.:153489-56-6
Molecular Formula:C₁₈H₃₁NO₂SSi
Molecular Weight:353.601
Hs Code.:

Synonyms:4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide

Suppliers and Price of 4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide

Chemical Property:

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Technology Process of 4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide

There total 3 articles about 4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: Carbonic acid methyl ester (R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl ester

: 4-Methyl-N-((E)-1-trimethylsilanyl-oct-1-enyl)-benzenesulfonamide

: 153489-56-6
4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide

Guidance literature:: With tributylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In acetonitrile; at 75 ℃; for 12h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)73814-7

Reference yield:

: Carbonic acid methyl ester (R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl ester

: 153489-56-6
4-Methyl-N-[(R)-1-((E)-2-trimethylsilanyl-vinyl)-hexyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: NaN₃, PBu₃ / Pd₂(dba)3*CHCl₃ / tetrahydrofuran; H₂O / 24 h / Ambient temperature

2: 1.) PPh₃

With sodium azide; tributylphosphine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In tetrahydrofuran; water;
DOI:10.1016/S0040-4039(00)73814-7