1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside

Base Information

• Chemical Name: 1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside
• CAS No.: 116113-83-8
• Molecular Formula: C₄₈H₅₆Cl₄O₂₂
• Molecular Weight: 1126.77

Synonyms:1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside

Chemical Property of 1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside

Chemical Property:

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Technology Process of 1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside

There total 2 articles about 1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

di-isopropyl azodicarboxylate (2446-83-5) + C24H28O7 (114828-03-4) → C32H42N2O10 (116135-14-9) + 1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside (116113-83-8)

Guidance literature:

With thiamine diphosphate; In tetrahydrofuran; for 0.25h; Ambient temperature;

DOI:10.1016/S0040-4039(00)96788-1

Reference yield: 30.0%

4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-D-glucopyranose (116113-81-6,116113-82-7) + C24H28O7 (114828-03-4) → C32H42N2O10 (116135-14-9) + 1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside (116113-83-8)

Guidance literature:

With di-isopropyl azodicarboxylate; thiamine diphosphate; In tetrahydrofuran; for 0.25h; Ambient temperature;

DOI:10.1016/S0040-4039(00)96788-1

Reference yield: 20.0%

1-O-phyllanthocinoyl 4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-β-D-glucopyranoside (116113-83-8) → (+)-phyllanthostatin 2 (81558-18-1)

Guidance literature:

With hydrazine dithiocarbonate; In tetrahydrofuran;

DOI:10.1016/S0040-4039(00)96788-1

upstream raw materials:

di-isopropyl azodicarboxylate

C₂₄H₂₈O₇

4,6-bis-O-(chloroacetyl)-3-O-acetyl-2-O-(2,4-bis-O-(chloroacetyl)-3-O-acetyl-6-deoxy-β-D-glucopyranosyl)-D-glucopyranose

Downstream raw materials:

(+)-phyllanthostatin 2

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