2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate

Base Information

• Chemical Name: 2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate
• CAS No.: 1242272-43-0
• Molecular Formula: C₃₅H₂₉BrO₈
• Molecular Weight: 657.514
• Mol file: 1242272-43-0.mol

Synonyms:2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate

Chemical Property of 2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate

Chemical Property:

Purity/Quality:

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Technology Process of 2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate

There total 1 articles about 2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoic acid (1242272-41-8) + 2-bromoethanol (540-51-2) → 2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate (1242272-43-0)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 10h;

DOI:10.1002/asia.200800391

Reference yield: 90.0%

3-{2'-(4''-dimethylaminophenyl)ethenyl}-4,4'-difluoro-8-(4-(3-azidopropoxy))-phenyl-1,3,5,7-tetramethyl-4-bora-3 a,4 a-diaza-s-indacene (1242274-59-4) + 2-bromoethyl-3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoate (1242272-43-0) → C159H161B4BrF8N24O12

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; at 20 ℃; for 10h; Inert atmosphere;

DOI:10.1002/asia.200800391

upstream raw materials:

3,5-bis(3,5-bis(2-propynyloxy)benzyloxy)benzoic acid

2-bromoethanol