carbacephalosporin hydrochloride

Base Information

Chemical Name:carbacephalosporin hydrochloride
CAS No.:123932-46-7
Molecular Formula:C₁₅H₁₄ClN₃O₅*ClH
Molecular Weight:388.207
Hs Code.:

Synonyms:carbacephalosporin hydrochloride

Suppliers and Price of carbacephalosporin hydrochloride

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Chemical Property of carbacephalosporin hydrochloride

Chemical Property:

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Technology Process of carbacephalosporin hydrochloride

There total 9 articles about carbacephalosporin hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 119892-46-5
p-nitrobenzyl 7β-[(phenoxyacetyl)amino]-3-hydroxy-1-carba-1-dethia-3-cephem-4-carboxylate

: 123932-46-7
carbacephalosporin hydrochloride

Guidance literature:: With hydrogenchloride; (PhO)3P*Cl₂; In pyridine; dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4039(01)80388-9

Reference yield:

: 99333-65-0
1-benzyl-3β-((S)-2-oxo-4-phenyloxazolidin-3-yl)-4β-[2-(2-furyl)ethyl]azetidin-2-one

: 123932-46-7
carbacephalosporin hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) Li/NH₃, t-BuOH 2.) aq. NaHCO₃ / 1.) THF 2.) CH₃CN

2: 77 percent / O₃, H₂O₂ / CH₂Cl₂; methanol

3: carbonyl diimidazole / tetrahydrofuran

4: 85 percent / p-dodecyl-SO₂N₃, TEA / acetonitrile

5: 72 percent / Rh₂(O₂CC₇H₁₅)4 / CH₂Cl₂

6: 72 percent / (PhO)3PCl₂, HCl / pyridine; CH₂Cl₂; ethyl acetate; various solvent(s)

With hydrogenchloride; (PhO)3P*Cl₂; p-dodecyl-SO₂N₃; TEA; ammonia; dihydrogen peroxide; lithium; sodium hydrogencarbonate; ozone; 1,1'-carbonyldiimidazole; tert-butyl alcohol; Rh₂(O₂CC₇H₁₅)4; In tetrahydrofuran; pyridine; methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/S0040-4039(01)80388-9

Reference yield:

: 124831-36-3
N-[(2R,3S)-2-(2-Furan-2-yl-ethyl)-4-oxo-azetidin-3-yl]-2-phenoxy-acetamide

: 123932-46-7
carbacephalosporin hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / O₃, H₂O₂ / CH₂Cl₂; methanol

2: carbonyl diimidazole / tetrahydrofuran

3: 85 percent / p-dodecyl-SO₂N₃, TEA / acetonitrile

4: 72 percent / Rh₂(O₂CC₇H₁₅)4 / CH₂Cl₂

5: 72 percent / (PhO)3PCl₂, HCl / pyridine; CH₂Cl₂; ethyl acetate; various solvent(s)

With hydrogenchloride; (PhO)3P*Cl₂; p-dodecyl-SO₂N₃; TEA; dihydrogen peroxide; ozone; 1,1'-carbonyldiimidazole; Rh₂(O₂CC₇H₁₅)4; In tetrahydrofuran; pyridine; methanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/S0040-4039(01)80388-9