allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside

Base Information

Chemical Name:allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside
CAS No.:213776-87-5
Molecular Formula:C₃₉H₄₂O₆
Molecular Weight:606.759
Hs Code.:

Synonyms:allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside

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Technology Process of allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside

There total 2 articles about allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 107-18-6
allyl alcohol

: 166828-15-5
4,5,6,8-tetra-O-benzyl-1,2-dideoxy-α-D-gluco-oct-1-eno-3-ulopyranose

: 213776-87-5
allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside

Guidance literature:: With 4 A molecular sieve; montmorillonite K-10; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(98)01247-7

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 213776-87-5
allyl (4,5,6,8-tetra-O-benzyl-1,2-dideoxy)-α-D-gluco-oct-1-eno-3-ulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / diethyl ether / -78 °C

2: 74 percent / Montmorillonite K-10 clay; 4 Angstroem molecular sieves / CH₂Cl₂ / 20 °C

With 4 A molecular sieve; Montmorillonite K-10 clay; In diethyl ether; dichloromethane;
DOI:10.1039/b401699h