4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime

Base Information

Chemical Name:4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime
CAS No.:1551093-24-3
Molecular Formula:C₁₇H₁₅F₃N₂O₄
Molecular Weight:368.312
Hs Code.:

Synonyms:4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime

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Chemical Property of 4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime

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Technology Process of 4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime

There total 1 articles about 4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3717-21-3,3717-22-4,3235-04-9,140461-28-5,140461-29-6
(E)-4-methoxybenzaldoxime

: 1422984-99-3
(E)-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)benzene

: 1551093-24-3
4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime

: C₁₇H₁₅F₃N₂O₄

Guidance literature:: With 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1S)-(6-methoxyquinolin-4-yl)(5-vinylquinuclidin-2-yl)methyl)thiourea; In acetonitrile; at 20 ℃; for 120h; Reagent/catalyst; Solvent; Temperature; Overall yield = 46 %; enantioselective reaction; Catalytic behavior;
DOI:10.1039/c3ob42329h

Reference yield: 78.0%

: 1551093-24-3
4-(E)-methoxybenzaldehyde O-(2S)-(1,1,1-trifluoro-3-nitro-2-phenylpropan-2-yl)oxime

: (2S)-3-amino-1,1,1-trifluoro-2-phenylpropan-2-ol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 25 ℃; for 24h; under 19001.3 Torr;
DOI:10.1039/c3ob42329h