{PdPtI₂(dppm)2}

Base Information

Chemical Name:{PdPtI₂(dppm)2}
CAS No.:82307-38-8
Molecular Formula:C₅₀H₄₄I₂P₄PdPt
Molecular Weight:1324.1
Hs Code.:

Synonyms:{PdPtI₂(dppm)2}

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Chemical Property of {PdPtI₂(dppm)2}

Chemical Property:

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Technology Process of {PdPtI₂(dppm)2}

There total 4 articles about {PdPtI₂(dppm)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: bis[μ-bis(diphenylphosphino)methane]-dichloropalladiumplatinum(Pd-Pt)

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 82307-38-8
{PdPtI₂(dppm)2}

Guidance literature:: In acetone; complex and NaI suspended in acetone and heated under reflux for 3 h; washing with H2O and acetone and drying in vac.; elem. anal.;
DOI:10.1039/DT9830000889

Reference yield: 54.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 82307-36-6
{PdPtCl₂(dppm)2}

: 14362-44-8,20461-54-5,69239-56-1
iodide

: 113109-37-8
PdPtCo₂(CO)7(dppm)2

: 82307-38-8
{PdPtI₂(dppm)2}

: 16887-00-6
chloride

Guidance literature:: In tetrahydrofuran; A THF soln. of Na{Co(CO)4} was added at 0°C to a mixt. of {PdPtCl2(dppm)2} and I(1-) in THF. After 2 h of react. at 0°C and 2 h of react. at room temp., the pale yellow soln. had turned brown-red.; Filtration and crystn. in THF/Et2O afforded a powder. The IR spectrum (in THF) of the green mother liquor revealed exclusively the presence of PdPtCo2(CO)7(dppm)2.;

Reference yield: 54.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 82307-36-6
{PdPtCl₂(dppm)2}

: 113109-37-8
PdPtCo₂(CO)7(dppm)2

: 82307-38-8
{PdPtI₂(dppm)2}

Guidance literature:: With potassium iodide; In tetrahydrofuran; A THF soln. of Na{Co(CO)4} was added at 0°C to a mixt. of {PdPtCl2(dppm)2} and KI in THF. After 2 h of react. at 0°C and 2 h of react. at room temp., the pale yellow soln. had turned brown-red.; Filtration and crystn. in THF/Et2O afforded PdPtI2(dppm)2 as a powder. The IR spectrum (in THF) of the green mother liquor revealed exclusively the presence of PdPtCo2(CO)7(dppm)2.;