Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆}

Base Information

Chemical Name:Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆}
CAS No.:155806-11-4
Molecular Formula:C₄₇H₄₅IrP₃*F₆P
Molecular Weight:1039.98
Hs Code.:

Ir(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)(C<sub>6</sub>H<sub>6</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>={Ir(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)(C<sub>6</sub>H<sub>6</sub>)}{PF<sub>6</sub>}

Synonyms:Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆}

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Chemical Property of Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆}

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Technology Process of Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆}

There total 1 articles about Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60969-19-9
thallium(I) hexafluorophosphate

: 154798-32-0
(CH₃C(CH₂P(C₆H₅)2)3)Ir((CH)4)(Cl)

: 74-86-2,25067-58-7
acetylene

: 155806-11-4
Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆}

Guidance literature:: In tetrahydrofuran; byproducts: TlCl; High Pressure; soln. of Ir-complex in THF is treated with ethyne in the presence of TlPF6 as chloride scavenger at room temp.; IR- and NMR-spectroscopy;
DOI:10.1021/om00016a020

Reference yield: 80.0%

: 155806-11-4
Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₆H₆)}{PF₆}

: 95-15-8,11095-43-5
Benzo[b]thiophene

: Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₈H₆S)⁽¹⁺⁾*PF₆^(1-)={Ir(CH₃C(CH₂P(C₆H₅)2)3)(C₈H₆S)}{PF₆}

Guidance literature:: In tetrahydrofuran; under N2; a soln. of the Ir complex and the benzothiophene in THF was refluxed for 20 h; addn. of ethanol, partial evapn., filtered, washed with ethanol and pentane; elem. anal.;
DOI:10.1021/ja00089a027