10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside

Base Information

Chemical Name:10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside
CAS No.:574737-34-1
Molecular Formula:C₃₃H₄₇N₃O₆
Molecular Weight:581.753
Hs Code.:

Synonyms:10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside

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Chemical Property of 10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside

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Technology Process of 10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside

There total 6 articles about 10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 574737-33-0
10-azidodecyl 3,4-O-isopropylidene-β-D-galactopyranoside

: 100-39-0
benzyl bromide

: 574737-34-1
10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 25 ℃; for 2h;
DOI:10.1016/j.tet.2005.03.102

Reference yield:

: 860036-11-9
10-azidodecyl β-D-galactopyranoside

: 574737-34-1
10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 392 mg / camphorsulfonic acid / acetone / 2.5 h / 25 °C

2: 100 percent / NaH / dimethylformamide / 2 h / 25 °C

With camphor-10-sulfonic acid; sodium hydride; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2005.03.102

Reference yield:

: 574737-31-8
10-bromodecyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

: 574737-34-1
10-azidodecyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / NaN₃ / dimethylformamide / 4 h / 80 °C

2: NaOMe / methanol / 3 h

3: 392 mg / camphorsulfonic acid / acetone / 2.5 h / 25 °C

4: 100 percent / NaH / dimethylformamide / 2 h / 25 °C

With sodium azide; camphor-10-sulfonic acid; sodium methylate; sodium hydride; In methanol; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2005.03.102