4-fluoro-2-(phenylcarbonyl)phenyl dimethylsulfamate

Base Information

• Chemical Name: 4-fluoro-2-(phenylcarbonyl)phenyl dimethylsulfamate
• CAS No.: 1259092-16-4
• Molecular Formula: C₁₅H₁₄FNO₄S
• Molecular Weight: 323.345
• Mol file: 1259092-16-4.mol

Synonyms:4-fluoro-2-(phenylcarbonyl)phenyl dimethylsulfamate

Chemical Property of 4-fluoro-2-(phenylcarbonyl)phenyl dimethylsulfamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-fluoro-2-(phenylcarbonyl)phenyl dimethylsulfamate

There total 1 articles about 4-fluoro-2-(phenylcarbonyl)phenyl dimethylsulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-fluorophenyl N,N-dimethylsulfamate (1259092-05-1) + benzoyl chloride (98-88-4) → 4-fluoro-2-(phenylcarbonyl)phenyl dimethylsulfamate (1259092-16-4)

Guidance literature:

4-fluorophenyl N,N-dimethylsulfamate; With tmp4Zr*4MgCl₂*6LiCl; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;

benzoyl chloride; With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at 0 ℃; for 1h; regioselective reaction; Inert atmosphere;

DOI:10.1002/anie.201003558

upstream raw materials:

4-fluorophenyl N,N-dimethylsulfamate

benzoyl chloride