(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal

Base Information

Chemical Name:(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal
CAS No.:93170-55-9
Molecular Formula:C₂₉H₂₈O₁₀S
Molecular Weight:568.601
Hs Code.:

Synonyms:(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal

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Technology Process of (2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal

There total 1 articles about (2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 72263-10-6
2L-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone

: 107-21-1
ethylene glycol

: 93170-55-9
(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal

Guidance literature:: With sulfuric acid; In 1,4-dioxane; benzene; for 5h; Heating;
DOI:10.1016/0008-6215(84)85276-3

Reference yield: 86.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 93170-55-9
(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal

: 93170-56-0
(2S)-(2,4,5/3)-2,3-dibenzoyloxy-4-toluene-p-sulphonyloxy-5-trifluoromethanesulphonyloxycyclohexanone ethylene acetal

Guidance literature:: With pyridine; In dichloromethane; at -40 - 10 ℃; for 3.5h;
DOI:10.1016/0008-6215(84)85276-3

Reference yield: 60.0%

: 93170-55-9
(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene acetal

: 93170-57-1
(2S)-(2/3)-2,3-dibenzoyloxycyclohex-4-enone ethylene acetal

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In toluene; acetonitrile; for 11h; Heating;
DOI:10.1016/0008-6215(84)85276-3