(+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate

Base Information

• Chemical Name: (+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate
• CAS No.: 78548-59-1
• Molecular Formula: C₁₀H₁₄Cl₂O₂
• Molecular Weight: 237.126

Synonyms:(+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate

Chemical Property of (+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of (+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate

There total 3 articles about (+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-) Trans Ethyl-3-(β,β-Dichloro-α-Tosyloxyethyl)-2,2-Dimethylcyclopropane-1-Carboxylate (63928-95-0) → (+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate (78548-59-1,60940-88-7)

Guidance literature:

With sodium hydroxide; In ethanol;

Reference yield:

diazoacetic acid ethyl ester (623-73-4) + 1,1-dichloro-4-methyl-penta-1,3-diene (55667-43-1) → (+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate (78548-59-1,60940-88-7) + (1S,3S)-3-(2,2-Dichloro-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid ethyl ester (78548-58-0,60940-88-7) + (1R,3R)-3-(2,2-Dichloro-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid ethyl ester (60940-88-7) + (1S,3R)-3-(2,2-Dichloro-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid ethyl ester (60940-88-7)

Guidance literature:

NaCuX-18 (zeolite) - (L-Ala)2; at 79.9 ℃; Yield given. Yields of byproduct given;

Reference yield:

→ (+/-) Trans Ethyl 3-(β,β-dichlorovinyl)-2,2-dimethylcyclopropane-1-carboxylate (78548-59-1,60940-88-7)

Guidance literature:

Diethyl-2,2-dimethyl-3-(2',2'-dichlorvinyl)-cyclopropan-1,1-dicarboxylat, Δ;

upstream raw materials:

diazoacetic acid ethyl ester

1,1-dichloro-4-methyl-penta-1,3-diene

(+/-) Trans Ethyl-3-(β,β-Dichloro-α-Tosyloxyethyl)-2,2-Dimethylcyclopropane-1-Carboxylate

Downstream raw materials:

3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylic acid

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