Technology Process of C28H39N5O3
There total 8 articles about C28H39N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: acetic acid; hydrazine hydrate / ethanol / 0.25 h / 140 °C / Microwave irradiation
1.2: 160 °C
2.1: trifluoroacetic acid / 1,4-dioxane / 20 °C
3.1: potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0) / water; 1,4-dioxane / 1 h / 100 °C / Inert atmosphere
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 20 °C
4.2: 16 h / 20 °C
5.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C
6.1: triethylamine / 2 h / 20 °C
7.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C
With
tris-(dibenzylideneacetone)dipalladium(0); lithium aluminium tetrahydride; sodium hydride; potassium carbonate; hydrazine hydrate; acetic acid; triethylamine; trifluoroacetic acid; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium 2-methylbutan-2-olate / tetrahydrofuran; toluene / 20 °C
1.2: 0.33 h / 20 °C
2.1: hydrazine hydrate / ethanol / 0.25 h / 140 °C / Microwave irradiation
3.1: trifluoroacetic acid / 1,4-dioxane / 20 °C
4.1: potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0) / water; 1,4-dioxane / 1 h / 100 °C / Inert atmosphere
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 20 °C
5.2: 16 h / 20 °C
6.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C
7.1: triethylamine / 2 h / 20 °C
8.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C
With
tris-(dibenzylideneacetone)dipalladium(0); lithium aluminium tetrahydride; sodium hydride; potassium 2-methylbutan-2-olate; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; toluene; mineral oil;