allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

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Chemical Name:allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside
CAS No.:63064-57-3
Molecular Formula:C₃₉H₅₀N₂O₁₄
Molecular Weight:770.831
Hs Code.:

Synonyms:allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

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Chemical Property of allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

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Technology Process of allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

There total 8 articles about allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 129437-72-5
allyl O-(3,4,6-tri-O-acetyl-2-chloroacetamido-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

: 63064-57-3
allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: With acetic acid; zinc; In various solvent(s); for 3h; Heating;
DOI:10.1016/0008-6215(90)84083-7

Reference yield:

: 54400-75-8
allyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 63064-57-3
allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: p-TosOH

2: 89 percent / NaBH₃CN

3: 44 percent / FeCl₃, molecular sieves (3 Angstroem) / CH₂Cl₂ / 30 h / Heating

4: 84 percent / zinc, acetic acid / various solvent(s) / 3 h / Heating

With 3 A molecular sieve; iron(III) chloride; sodium cyanoborohydride; toluene-4-sulfonic acid; acetic acid; zinc; In dichloromethane;
DOI:10.1016/0008-6215(90)84083-7

Reference yield:

: 63064-49-3
allyl 2-acetamido-2-deoxy-4,6-O-benzylidene-α-D-glucopyranoside

: 63064-57-3
allyl O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaBH₃CN

2: 44 percent / FeCl₃, molecular sieves (3 Angstroem) / CH₂Cl₂ / 30 h / Heating

3: 84 percent / zinc, acetic acid / various solvent(s) / 3 h / Heating

With 3 A molecular sieve; iron(III) chloride; sodium cyanoborohydride; acetic acid; zinc; In dichloromethane;
DOI:10.1016/0008-6215(90)84083-7