3-Chloro-10,11-dihydro-5H-dibenzo azepine

Base Information

Chemical Name:3-Chloro-10,11-dihydro-5H-dibenzo azepine
CAS No.:39607-90-4
Molecular Formula:C₁₄H₁₀ClN
Molecular Weight:227.693
Hs Code.:
Mol file:39607-90-4.mol

Synonyms:3-chloro-5H-dibenzo[b,f]azepine

Suppliers and Price of 3-Chloro-10,11-dihydro-5H-dibenzo azepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-Chloro-10,11-dihydro-5H-dibenzo azepine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Chloro-10,11-dihydro-5H-dibenzo azepine

There total 8 articles about 3-Chloro-10,11-dihydro-5H-dibenzo azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1-(3-chlorophenyl)-1H-indole

: 39607-90-4
3-chloro-5H-dibenzo[b,f]azepine

Guidance literature:: With polyphosphoric acid; at 100 ℃; for 12h; Inert atmosphere;

Reference yield: 12.6%

: 1-(3-chlorophenyl)-1H-indole

: 39607-90-4
3-chloro-5H-dibenzo[b,f]azepine

: C₁₄H₁₀ClN

Guidance literature:: With polyphosphoric acid; at 100 ℃; for 12h; Inert atmosphere;

Reference yield:

: 625-99-0
3-iodochlorobenzene

: 39607-90-4
3-chloro-5H-dibenzo[b,f]azepine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; copper / nitrobenzene / 12 h / 210 °C / Inert atmosphere

2: polyphosphoric acid / 12 h / 100 °C / Inert atmosphere

With copper; potassium carbonate; In nitrobenzene;