N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

Base Information

Chemical Name:N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]
CAS No.:947406-13-5
Molecular Formula:C₃₅H₄₅N₉O₆
Molecular Weight:687.799
Hs Code.:

N<sup>α</sup>-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

Synonyms:N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

Suppliers and Price of N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

Chemical Property:

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Technology Process of N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

There total 3 articles about N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 947406-12-4
N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine methyl ester]

: 947406-13-5
N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

Guidance literature:: With hydrazine hydrate; In methanol; for 5h; Heating;
DOI:10.1002/ardp.200600187

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 947406-13-5
N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethyl chloroformate; Et₃N / CH₂Cl₂ / 0.17 h / -20 °C

1.2: 76 percent / CH₂Cl₂ / -20 - 20 °C

2.1: 70 percent / hydrazine hydrate / methanol / 5 h / Heating

With chloroformic acid ethyl ester; hydrazine hydrate; triethylamine; In methanol; dichloromethane;
DOI:10.1002/ardp.200600187

Reference yield:

: 96844-89-2
N,N'-bis<(1S)-1-carboxy-2-methylpropyl>-2,6-bis(aminocarbonyl)pyridine

: 947406-13-5
N^α-dipicolinoyl-bis-[L-valyl-L-phenylalanine hydrazide]

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethyl chloroformate; Et₃N / CH₂Cl₂ / 0.17 h / -20 °C

1.2: 76 percent / CH₂Cl₂ / -20 - 20 °C

2.1: 70 percent / hydrazine hydrate / methanol / 5 h / Heating

With chloroformic acid ethyl ester; hydrazine hydrate; triethylamine; In methanol; dichloromethane;
DOI:10.1002/ardp.200600187