2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid

Base Information

Chemical Name:2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid
CAS No.:914298-27-4
Molecular Formula:C₂₀H₂₀ClNO₇
Molecular Weight:421.834
Hs Code.:

Synonyms:2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid

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Chemical Property of 2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid

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Technology Process of 2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid

There total 6 articles about 2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 914298-94-5
2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid methyl ester

: 914298-27-4
2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid

Guidance literature:: 2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid methyl ester; With lithium hydroxide; water; In methanol; at 40 ℃; for 12h;

With sodium acetate; acetic acid; In methanol; water;

Reference yield:

: 444607-92-5
2-(tert-butyl) 1-methyl isoindoline-1,2-dicarboxylate

: 914298-27-4
2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 12 h / 20 °C

2.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

3.1: methanol; lithium hydroxide; water / 12 h / 40 °C

3.2: NaOAc-HOAc buffer

With 4-methyl-morpholine; hydrogenchloride; methanol; lithium hydroxide; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 914298-92-3
methyl 2,4-dimethoxymethyloxybenzoate

: 914298-27-4
2-(5-chloro-2,4-bis-methoxymethoxybenzoyl)-2,3-dihydro-1H-isoindole-1-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: calcium hypochlorite / acetic acid; acetone / 12 h / 20 °C

2.1: methanol; sodium hydroxide; water / 12 h / 20 °C

2.2: pH 6.5

3.1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C

4.1: methanol; lithium hydroxide; water / 12 h / 40 °C

4.2: NaOAc-HOAc buffer

With 4-methyl-morpholine; methanol; lithium hydroxide; sodium hydroxide; calcium hypochlorite; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetic acid; N,N-dimethyl-formamide; acetone;