benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate

Base Information

Chemical Name:benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate
CAS No.:188950-58-5
Molecular Formula:C₇₇H₁₀₃O₁₅P
Molecular Weight:1299.63
Hs Code.:

Synonyms:benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate

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Chemical Property of benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate

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Technology Process of benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate

There total 5 articles about benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphorous acid benzyl ester (1R,2R,3R,4R,5S,6R)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(4-methoxy-benzyloxy)-cyclohexyl ester (R)-2,3-bis-undec-10-enyloxy-propyl ester

: 188950-58-5
benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; Yield given; 1.) -40 deg C, 5 min, 2.) from 0 deg C to RT, 60 min;
DOI:10.1002/(SICI)1099-1344(199703)39:3<251::AID-JLCR964>3.0.CO;2-Y

Reference yield:

: 7766-50-9
1-undecen-11-ylbromide

: 188950-58-5
benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / NaH / dimethylformamide / 2 h / Ambient temperature

2: 98 percent / DDQ / CH₂Cl₂ / 3 h / Ambient temperature

3: 95 percent / i-Pr₂NEt / CH₂Cl₂ / 1.42 h / 0 - 20 °C

4: 1H-tetrazole / CH₂Cl₂ / 2 h / Ambient temperature

5: m-CPBA / CH₂Cl₂ / 1.) -40 deg C, 5 min, 2.) from 0 deg C to RT, 60 min

With 1H-tetrazole; sodium hydride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1099-1344(199703)39:3<251::AID-JLCR964>3.0.CO;2-Y

Reference yield:

: 188950-56-3
1,2-di-(10-undecenyl)-sn-glycerol

: 188950-58-5
benzyl 3-[1,2-di-(10-undecenyl)-sn-glyceryl] 1-[2,6-di-O-benzoxymethyl-3-O-benzyl-4,5-O-(p-methoxybenzyl)-D-myo-inosityl] phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / i-Pr₂NEt / CH₂Cl₂ / 1.42 h / 0 - 20 °C

2: 1H-tetrazole / CH₂Cl₂ / 2 h / Ambient temperature

3: m-CPBA / CH₂Cl₂ / 1.) -40 deg C, 5 min, 2.) from 0 deg C to RT, 60 min

With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1002/(SICI)1099-1344(199703)39:3<251::AID-JLCR964>3.0.CO;2-Y