ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate

Base Information

Chemical Name:ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate
CAS No.:119047-45-9
Molecular Formula:C₂₄H₃₀O₄
Molecular Weight:382.5
Hs Code.:

Synonyms:ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate

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Chemical Property of ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate

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Technology Process of ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate

There total 4 articles about ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 31469-16-6
1-ethoxy-1-((trimethylsilyl)oxy)-2-methylpropene

: 119047-51-7,119047-52-8
1ξ-acetoxy-6-methoxy-2ξ-(p-methoxyphenyl)-1,2,3,4-tetrahydronaphthalene

: 119047-45-9
ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate

Guidance literature:: With zinc(II) iodide; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1071/CH9880745

Reference yield: 83.0%

: 119047-42-6
ethyl 2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-3',4'-dihydronaphthalen-1'-yl>propanoate

: 119047-45-9
ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; at 60 ℃; for 12h; under 5320 Torr;
DOI:10.1071/CH9880745

Reference yield:

: 31469-16-6
1-ethoxy-1-((trimethylsilyl)oxy)-2-methylpropene

: 119047-45-9
ethyl (1'RS,2'RS)-2-methyl-2-<6'-methoxy-2'-(p-methoxyphenyl)-1',2',3',4'-tetrahydronaphthalen-1'-yl>propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / titanium tetrachloride / CH₂Cl₂ / 24 h / Ambient temperature

2: 83 percent / H₂ / 10percent palladium/charcoal / acetic acid / 12 h / 60 °C / 5320 Torr

With hydrogen; titanium tetrachloride; palladium on activated charcoal; In dichloromethane; acetic acid;
DOI:10.1071/CH9880745