2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride

Base Information

Chemical Name:2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride
CAS No.:81440-84-8
Molecular Formula:C₁₇H₂₀INO₃S*ClH
Molecular Weight:481.782
Hs Code.:

Synonyms:2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride

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Chemical Property of 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride

Chemical Property:

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Technology Process of 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride

There total 3 articles about 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Benzenesulfonic acid 2-(tert-butoxycarbonylamino-methyl)-4-tert-butyl-6-iodo-phenyl ester

: 81440-84-8
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; at 20 - 25 ℃; for 3h; Yield given;
DOI:10.1021/jm00348a024

Reference yield:

: 58456-91-0
2-aminomethyl-4-tert-butyl-6-iodophenol

: 81440-84-8
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / Et₃N / tetrahydrofuran; H₂O / 24 h / 60 - 65 °C

2: Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

3: conc. HCl / ethanol / 3 h / 20 - 25 °C

With hydrogenchloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm00348a024

Reference yield:

: 68967-65-7
1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

: 81440-84-8
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl benzenesulfonate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

2: conc. HCl / ethanol / 3 h / 20 - 25 °C

With hydrogenchloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm00348a024