C₅₄H₄₆O₈

Base Information

Chemical Name:C₅₄H₄₆O₈
CAS No.:83487-65-4
Molecular Formula:C₅₄H₄₆O₈
Molecular Weight:822.954
Hs Code.:

C<sub>54</sub>H<sub>46</sub>O<sub>8</sub>

Synonyms:C₅₄H₄₆O₈

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Chemical Property of C₅₄H₄₆O₈

Chemical Property:

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Technology Process of C₅₄H₄₆O₈

There total 12 articles about C₅₄H₄₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 83487-64-3
C₄₈H₄₂O₈

: 106-96-7
propargyl bromide

: 83487-65-4
C₅₄H₄₆O₈

Guidance literature:: With potassium carbonate; In acetone; for 45h; Heating;
DOI:10.1021/ja00389a050

Reference yield:

: 83511-07-3
3,7-dihydroxy-2-naphthoic acid

: 83487-65-4
C₅₄H₄₆O₈

Guidance literature:: Multi-step reaction with 7 steps

1: 52 percent / NaHCO₃ / dimethylformamide / 1 h / 70 °C

2: 80 percent / K₂CO₃ / acetone / 11 h / Heating

3: 1.) n-BuLi, 2.) KOH / 1.) 0 deg C, 1 h; room temperature, overnight, 2.) MeOH, reflux, 4 h

4: 99 percent / 4-(dimethylamino)pyridine, cyclohexyl carbodiimide / CH₂Cl₂ / 3 h / Ambient temperature

5: 93 percent / HCl gas / benzene / 0.07 h

6: 87 percent / cupric acetate monohydrate / pyridine / 2.5 h / 40 °C

7: 66 percent / K₂CO₃ / acetone / 45 h / Heating

With hydrogenchloride; dmap; potassium hydroxide; n-butyllithium; N-cyclohexylcarbodiimide; copper diacetate; sodium hydrogencarbonate; potassium carbonate; In pyridine; dichloromethane; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/ja00389a050

Reference yield:

: 26513-28-0
sodium 2-carboxy-3-hydroxy-7-naphthalenesulfonate

: 83487-65-4
C₅₄H₄₆O₈

Guidance literature:: Multi-step reaction with 8 steps

1: 81 percent / KOH / 1.5 h / 250 - 300 °C

2: 52 percent / NaHCO₃ / dimethylformamide / 1 h / 70 °C

3: 80 percent / K₂CO₃ / acetone / 11 h / Heating

4: 1.) n-BuLi, 2.) KOH / 1.) 0 deg C, 1 h; room temperature, overnight, 2.) MeOH, reflux, 4 h

5: 99 percent / 4-(dimethylamino)pyridine, cyclohexyl carbodiimide / CH₂Cl₂ / 3 h / Ambient temperature

6: 93 percent / HCl gas / benzene / 0.07 h

7: 87 percent / cupric acetate monohydrate / pyridine / 2.5 h / 40 °C

8: 66 percent / K₂CO₃ / acetone / 45 h / Heating

With hydrogenchloride; dmap; potassium hydroxide; n-butyllithium; N-cyclohexylcarbodiimide; copper diacetate; sodium hydrogencarbonate; potassium carbonate; In pyridine; dichloromethane; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/ja00389a050