6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide

Base Information

Chemical Name:6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide
CAS No.:145047-55-8
Molecular Formula:C₁₃H₅F₂NO₃
Molecular Weight:261.184
Hs Code.:

6,9-difluorobenzo<g>isoquinoline-5,10-dione 2-oxide

Synonyms:6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide

Suppliers and Price of 6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide

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Technology Process of 6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide

There total 1 articles about 6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4664-08-8
cinchomeronic anhydride

: 145047-55-8
6,9-difluorobenzoisoquinoline-5,10-dione 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) AlCl₃, 2.) f.H₂SO₄ / 1.) reflux, 22 h, 2.) from 135 to 140 deg C, 3 h

2: m-chloroperoxybenzoic acid / CH₂Cl₂ / 24 h / Ambient temperature

With aluminium trichloride; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00032a018