(E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol

Base Information

Chemical Name:(E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol
CAS No.:73454-39-4
Molecular Formula:C₃₁H₄₄O₂S
Molecular Weight:480.755
Hs Code.:

Synonyms:(E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol

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Chemical Property of (E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol

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Technology Process of (E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol

There total 10 articles about (E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 73454-38-3
methyl (E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexanoate

: 73454-39-4
(E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; 1) 4.5h reflux 2) 2h at r.t.;
DOI:10.1021/jo01301a028

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 73454-39-4
(E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

2: 94 percent / LiAlH₄ / tetrahydrofuran / 1) 4.5h reflux 2) 2h at r.t.

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo01301a028

Reference yield:

: 106-24-1
Geraniol

: 73454-39-4
(E)-6-benzyloxy-5,5-dimethyl-2-(3,7-dimethyl-2,6-octadien-1-yl)-2-phenylthio-hexan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / PBr₃ / hexane / 0.33 h / 0 °C

3: 94 percent / LiAlH₄ / tetrahydrofuran / 1) 4.5h reflux 2) 2h at r.t.

With lithium aluminium tetrahydride; phosphorus tribromide; In tetrahydrofuran; hexane;
DOI:10.1021/jo01301a028