benzyloxycarbonylleucine 2-phenylethylamide

Base Information

Chemical Name:benzyloxycarbonylleucine 2-phenylethylamide
CAS No.:123709-00-2
Molecular Formula:C₂₂H₂₈N₂O₃
Molecular Weight:368.476
Hs Code.:

Synonyms:benzyloxycarbonylleucine 2-phenylethylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyloxycarbonylleucine 2-phenylethylamide

Chemical Property:

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Technology Process of benzyloxycarbonylleucine 2-phenylethylamide

There total 1 articles about benzyloxycarbonylleucine 2-phenylethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2018-66-8
Z-Leu-OH

: 64-04-0
phenethylamine

: 123709-00-2
benzyloxycarbonylleucine 2-phenylethylamide

Guidance literature:: With 1-ethyl-piperidine; chloroformic acid ethyl ester; Yield given. Multistep reaction; 1. CH₂Cl₂, 0 deg C, 15 min, 2. 0 deg C, 1 h, room temperature, 12 h;

Reference yield:

: 123709-00-2
benzyloxycarbonylleucine 2-phenylethylamide

: 87176-71-4
L-leucine N-phenethylamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; toluene; for 0.333333h; under 15001.2 Torr;

Reference yield:

: 123709-00-2
benzyloxycarbonylleucine 2-phenylethylamide

: 123709-03-5
L-alanyl-L-alanyl-L-leucine 2-phenylethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / toluene; methanol / 0.33 h / 15001.2 Torr

2: 1. N-hydroxysuccinimide, DCC / 1. DMF, THF, 0 deg C, 1 h; 2. room temperature, 12 h

3: 90 percent / H₂ / Pd/C / methanol / 0.67 h / 15001.2 Torr

With 1-hydroxy-pyrrolidine-2,5-dione; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; toluene;