3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one

Base Information

Chemical Name:3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one
CAS No.:1356832-74-0
Molecular Formula:C₂₃H₂₅NO₈S
Molecular Weight:475.519
Hs Code.:

Synonyms:3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one

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Chemical Property of 3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one

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Technology Process of 3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one

There total 2 articles about 3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 58734-19-3
3-methoxy-N-(4-methylbenzenesulfonyl)benzenecarboxamide

: 623-91-6
diethyl Fumarate

: 1356832-74-0
3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In toluene; at 130 ℃; for 48h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c2cc16963k

Reference yield:

: 623-73-4
diazoacetic acid ethyl ester

: 58734-19-3
3-methoxy-N-(4-methylbenzenesulfonyl)benzenecarboxamide

: 1356832-74-0
3-ethoxycarbonyl-3-ethoxycarbonylmethyl-6-methoxy-2-tosylisoindolin-1-one

: 1414971-17-7
C₂₃H₂₅NO₈S

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In toluene; at 130 ℃; for 48h; Overall yield = 70 %; Inert atmosphere;
DOI:10.1016/j.tet.2012.08.095