tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate

Base Information

Chemical Name:tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate
CAS No.:442913-31-7
Molecular Formula:C₃₁H₃₈N₂O₃
Molecular Weight:486.654
Hs Code.:

Synonyms:tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate

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Chemical Property of tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate

There total 2 articles about tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 103-67-3
benzyl-methyl-amine

: 442913-30-6
tert-butyl (2S)-2-[(1,1-diphenylmethylidene)amino]-4-[(2S)-oxiran-2-yl]butanoate

: 442913-31-7
tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate

Guidance literature:: In methanol; at 20 ℃; for 13h;
DOI:10.1021/ol026101e DOI:10.1002/hlca.200290026

Reference yield:

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 442913-31-7
tert-butyl (2S,5S)-2-[(1,1-diphenylmethylidene)amino]-5-hydroxy-6-[methyl(phenylmethyl)amino]hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / 9-anthracenylmethyl-chinchonidinium bromide / 18 h / -60 °C

2: 98 percent / methanol / 13 h / 20 °C

9-anthracenylmethyl-chinchonidinium bromide; In methanol;
DOI:10.1002/hlca.200290026