2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone

Base Information

Chemical Name:2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone
CAS No.:1427549-82-3
Molecular Formula:C₂₆H₂₀ClN₃O₅
Molecular Weight:489.915
Hs Code.:

Synonyms:2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone

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Chemical Property of 2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone

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Technology Process of 2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone

There total 5 articles about 2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 1427549-64-1
4-[(3,5-dimethyl-1H-pyrazol-1-yl)carbonyl]-1-(3-hydroxyphenyl)pyrrolidin-2-one

: 1427549-82-3
2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone

Guidance literature:: With sodium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h;
DOI:10.3390/molecules171214434

Reference yield:

: 91891-24-6
N-(3-hydroxyphenyl)-2-oxopyrrolidine-4-carboxylic acid

: 1427549-82-3
2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 5 h / Reflux

2: hydrazine hydrate / isopropyl alcohol / 5 h / Reflux

3: hydrogenchloride / isopropyl alcohol / 6 h / Reflux

4: sodium carbonate / dimethyl sulfoxide / 24 h / 20 °C

With hydrogenchloride; sulfuric acid; sodium carbonate; hydrazine hydrate; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.3390/molecules171214434

Reference yield:

: 105041-77-8
1-(3-hydroxyphenyl)-5-oxo-3-pyrrolidinecarbohydrazide

: 1427549-82-3
2-chloro-3-{3-[4-(3,5-dimethylpyrazole-1-carbonyl)-2-oxopyrrolidin-1-yl]phenoxy}-[1,4]naphthoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / isopropyl alcohol / 6 h / Reflux

2: sodium carbonate / dimethyl sulfoxide / 24 h / 20 °C

With hydrogenchloride; sodium carbonate; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.3390/molecules171214434