Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))⁽¹⁺⁾*SbF₆^(1-)=[Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))]SbF₆

Base Information

• Chemical Name: Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))⁽¹⁺⁾*SbF₆^(1-)=[Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))]SbF₆
• CAS No.: 170891-73-3
• Molecular Formula: C₅₀H₄₈IrN₂OP₂*F₆Sb
• Molecular Weight: 1182.85

Synonyms:Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))⁽¹⁺⁾*SbF₆^(1-)=[Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))]SbF₆

Chemical Property of Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))⁽¹⁺⁾*SbF₆^(1-)=[Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))]SbF₆

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Technology Process of Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))⁽¹⁺⁾*SbF₆^(1-)=[Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))]SbF₆

There total 1 articles about Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))⁽¹⁺⁾*SbF₆^(1-)=[Ir(H)2(P(C₆H₅)3)2(C₉H₆N(HNCOC(CH₃)3))]SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

{IrH2(acetone)2(PPh3)2}SbF6 (110077-68-4,89509-77-3) + α,α,α-trimethyl-N-(quinolin-8-yl)acetamide (170891-76-6) → Ir(H)2(P(C6H5)3)2(C9H6N(HNCOC(CH3)3))(1+)*SbF6(1-)=[Ir(H)2(P(C6H5)3)2(C9H6N(HNCOC(CH3)3))]SbF6 (170891-73-3)

Guidance literature:

In dichloromethane; N2-atmosphere; equimolar amts., room temp., 3 min; concn., pptn. on Et2O addn.; elem. anal.;

DOI:10.1021/ic00129a014

Reference yield: 64.0%

Ir(H)2(P(C6H5)3)2(C9H6N(HNCOC(CH3)3))(1+)*SbF6(1-)=[Ir(H)2(P(C6H5)3)2(C9H6N(HNCOC(CH3)3))]SbF6 (170891-73-3) → Ir(H)2(P(C6H5)3)2(C9H6N(NCOC(CH3)3)) (170891-68-6)

Guidance literature:

With Et₃N; In dichloromethane; N2-atmosphere; stirring (20°C, 10 min); concn., pptn. on Et2O addn.; elem. anal.;

DOI:10.1021/ic00129a014

upstream raw materials:

{IrH₂(acetone)2(PPh₃)2}SbF₆

α,α,α-trimethyl-N-(quinolin-8-yl)acetamide

Downstream raw materials:

Ir(H)2(P(C₆H₅)3)2(C₉H₆N(NCOC(CH₃)3))

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