methylbis(2,4,6-triisopropylphenyl)germane

Base Information

Chemical Name:methylbis(2,4,6-triisopropylphenyl)germane
CAS No.:141376-84-3
Molecular Formula:C₃₁H₅₀Ge
Molecular Weight:495.328
Hs Code.:

Synonyms:methylbis(2,4,6-triisopropylphenyl)germane

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Chemical Property of methylbis(2,4,6-triisopropylphenyl)germane

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Technology Process of methylbis(2,4,6-triisopropylphenyl)germane

There total 1 articles about methylbis(2,4,6-triisopropylphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 141376-82-1
bis(2,4,6-triisopropylphenyl)germane

: 77-78-1
dimethyl sulfate

: 141376-84-3
methylbis(2,4,6-triisopropylphenyl)germane

Guidance literature:: With hydrogenchloride; tert.-butyl lithium; In tetrahydrofuran; addn. of t-BuLi in pentanes to a soln. of the diarylgermane in THF at -23°C under dry Ar, stirring (1 h), dropwise addn. of the bright yellow soln. to a soln. of (CH3)2SO4 in THF at room temp., further stirring (4 h), addn. of 6 M HCl; extg. (Et2O), drying the org. layer (over MgSO4), filtration, removing solvent, chromy.;
DOI:10.1021/om00042a035