(3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide

Base Information

Chemical Name:(3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide
CAS No.:1446307-76-1
Molecular Formula:Br*C₂₈H₃₅N₂O₃
Molecular Weight:527.501
Hs Code.:

Synonyms:(3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide

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Chemical Property of (3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide

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Technology Process of (3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide

There total 2 articles about (3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1446307-75-0
(R)-quinuclidin-3-yl 2-phenyl-2-(piperidin-1-yl)acetate

: 70-11-1
α-bromoacetophenone

: 1446307-76-1
(3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide

Guidance literature:: In ethyl acetate; at 20 ℃; for 3h;

Reference yield:

: 25333-42-0
(R)-quinuclidin-3-ol

: 1446307-76-1
(3R)-1-(2-oxo-2-phenylethyl)-3-(2-phenyl-2-(piperidin-1-yl)acetoxy)-1-azonia bicyclo[2.2.2]octane bromide

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / tetrahydrofuran / 20 °C

2: ethyl acetate / 3 h / 20 °C

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;