C₂₂H₂₄O₈

Base Information

Chemical Name:C₂₂H₂₄O₈
CAS No.:1375644-97-5
Molecular Formula:C₂₂H₂₄O₈
Molecular Weight:416.428
Hs Code.:

C<sub>22</sub>H<sub>24</sub>O<sub>8</sub>

Synonyms:C₂₂H₂₄O₈

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Chemical Property of C₂₂H₂₄O₈

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Technology Process of C₂₂H₂₄O₈

There total 8 articles about C₂₂H₂₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1375645-35-4
C₂₂H₂₆O₈

: 1375644-97-5
C₂₂H₂₄O₈

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1016/j.tetlet.2012.03.098

Reference yield:

: 1375645-00-3
C₂₂H₂₆O₆

: 1375644-97-5
C₂₂H₂₄O₈

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; isopropyl alcohol / 8 h / 0 - 20 °C

2: Dess-Martin periodane / dichloromethane / 5 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; Dess-Martin periodane; In dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.tetlet.2012.03.098

Reference yield:

: 1375645-24-1
3-bromomethyl-4-iodofuran

: 1375644-97-5
C₂₂H₂₄O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C

1.2: 2 h / 70 °C

2.1: dmap; water; sodium chloride / dimethyl sulfoxide / 19 h / 180 °C

3.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / dichloromethane / 0.5 h / 20 °C

3.2: 1 h / 80 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

5.1: sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 20 °C

5.2: 20 °C

6.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 0.5 h / 0 °C

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; isopropyl alcohol / 8 h / 0 - 20 °C

8.1: Dess-Martin periodane / dichloromethane / 5 h / 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2-methyl-6-nitrobenzoic anhydride; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; sodium hydride; Dess-Martin periodane; sodium chloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol; 2.1: Krapcho decarboalkoxylation / 3.2: Stille coupling;
DOI:10.1016/j.tetlet.2012.03.098