5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate

Base Information

Chemical Name:5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate
CAS No.:816426-25-2
Molecular Formula:C₄₁H₄₁O₉P
Molecular Weight:708.745
Hs Code.:

Synonyms:5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate

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Chemical Property of 5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate

Chemical Property:

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Technology Process of 5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate

There total 3 articles about 5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 816426-23-0
5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-3-diphenylphosphate-1-O-thiocarbonic acid phenyl ester

: 816426-25-2
5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Heating;
DOI:10.1021/ja047360x

Reference yield:

: 474404-92-7
(+)-2,4,6-tri-O-benzyl-myo-inositol-3-phosphate

: 816426-25-2
5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 2.5 h

2: triethylamine; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 4 h

3: AIBN; Bu₃SnH / toluene / 2 h / Heating

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ja047360x

Reference yield:

: 816426-24-1
2,4,6-tri-O-benzyl-D-myo-inositol-3-diphenylphosphate-1-O-thiocarbonic acid phenyl ester

: 816426-25-2
5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-diphenylphosphate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 4 h

2: AIBN; Bu₃SnH / toluene / 2 h / Heating

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ja047360x