Dipp₂nacnacAlI₂

Base Information

Chemical Name:Dipp₂nacnacAlI₂
CAS No.:325465-26-7
Molecular Formula:C₂₉H₄₁AlI₂N₂
Molecular Weight:698.448
Hs Code.:

Synonyms:Dipp₂nacnacAlI₂

Suppliers and Price of Dipp₂nacnacAlI₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Dipp₂nacnacAlI₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Dipp₂nacnacAlI₂

There total 1 articles about Dipp₂nacnacAlI₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene)AlMe₂

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 325465-26-7
Dipp₂nacnacAlI₂

Guidance literature:: In toluene; byproducts: CH3I; mixed (at room temp.), stirred (at room temp. for three days), concd., stored (at -30°C, overnight);
DOI:10.1002/1521-3773(20001201)39:23<4274::AID-ANIE4274>3.0.CO;2-K

Reference yield: 70.0%

: 325465-26-7
Dipp₂nacnacAlI₂

: 501-65-5
diphenyl acetylene

: HC[(CMe)(N(2,6-i-Pr2C6H3))]2Al[η2-C2(C6H5)2]

Guidance literature:: With potassium; In toluene; byproducts: KI; a mixt. in toluene was stirred at room temp. for 2 d (inert atm.); volatiled were removed under vac., the residue was extd. with n-hexane, filtered, concd., stored at -30°C overnight;
DOI:10.1021/ja003185i

Reference yield: 69.0%

: 325465-26-7
Dipp₂nacnacAlI₂

: 3585-33-9
lithium dimethylamide

: 1018986-33-8
HC[C(Me)N(2,6-iPr₂C₆H₃)]2Al(I)NMe₂

Guidance literature:: In toluene; under N2 atm. soln. LiNMe2 in toluene was added at -78°C to soln.Al complex in toluene, allowed to warm to room temp. and stirred overni ght; volatiles were removed in vacuo, residue was extd. with Et2O and evapd. to dryness; elem. anal.;
DOI:10.1021/ic701896r