(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

Base Information

Chemical Name:(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate
CAS No.:773894-74-9
Molecular Formula:C₂₀H₂₆N₂O₆
Molecular Weight:390.436
Hs Code.:

Synonyms:(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

Suppliers and Price of (2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

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Technology Process of (2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

There total 1 articles about (2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 773894-71-6
(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-azidooctahydroindole-1,2,7-tricarboxylate

: 773894-74-9
(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

Guidance literature:: With zinc; In tetrahydrofuran; acetic acid; for 0.75h;
DOI:10.1021/ol048585f

Reference yield: 62.0%

: 773894-74-9
(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

: 55135-66-5
9-bromo-9-phenyl-9H-fluorene

: 773894-72-7
(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-(9-phenyl-9H-fluoren-9-ylamino)-octahydroindole-1,2,7-tricarboxylate

Guidance literature:: With lead(II) nitrate; triethylamine; In dichloromethane; for 20h;
DOI:10.1021/ol048585f

Reference yield:

: 773894-74-9
(2S,4R,7R,9R)-1-benzyl-2,7-dimethyl-7-aminooctahydroindole-1,2,7-tricarboxylate

: 773894-73-8
(2S,3aR,6R,7aR)-2-((3S,5S)-5-Carbamoyl-3-methoxycarbonyl-pyrrolidin-3-ylcarbamoyl)-6-{[(3S,5S,8S)-8-(4-hydroxy-benzyl)-7,10-dioxo-2,6,9-triaza-spiro[4.5]decane-3-carbonyl]-amino}-octahydro-indole-6-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / Pb(NO₃)2; Et₃N / CH₂Cl₂ / 20 h

2: 86 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 24 h

With lithium hydroxide; lead(II) nitrate; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol048585f